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Beilstein J. Org. Chem. 2018, 14, 1854–1858, doi:10.3762/bjoc.14.159
Graphical Abstract
Scheme 1: Previously reported preparation of IBS (1) [17].
Scheme 2: Oxidation of 2-iodobenzenesulfonate 5 by Oxone in water.
Figure 1: X-ray structure of an independent crystal unit of IBS 6-K.
Figure 2: Simplified representation of structure 6-K. Selected interatomic distances (Å): I(1)=O(1) 1.79; I(1...
Scheme 3: Comparison of the oxidation of sodium 2-iodobenzenesulfonate (5) with NaIO4 and 2-iodobenzenesulfon...